触媒反応には透明なパイレックス製の反応セルを用いた。各温度で熱処理した

触媒反応には透明なパイレックス製の反応セルを用いた。各温度で熱処理したリボン5 cmをHF処理し、蒸留水で洗浄させ、反応セルに移し、真空中で十分に乾燥させた後に、各種処理（酸素・水素処理）を行った。
反応セルのArパージ後、反応液を注入し、303 Kのオイルバスに浸けて反応を開始した。なお反応中は5 cc / minで水素をバブリングさせ、マグネティックスターラーを用いて撹拌した。また反応液は基質のオクテン1 mM、溶媒のメタノール5 ml、分析の標準物質となるビフェニル0.65 mMをマグネティックスターラーで10分間攪拌した後に使用した。1 h、2 h、4 h後に反応液をシリンジで取り出し、シリンジフィルターで触媒を除去してオートインジェクター用のサンプル管に移し、成分を分析した。
そして反応液の分析には2.5.3に示すGCを用いた。

ผลลัพธ์ (อังกฤษ) 1:

Using a catalytic reaction is a transparent made of Pyrex reaction cell. Ribbon 5 cm heat treatment temperature in HF, and washed with distilled water, transferred in the reaction cell the well dried in a vacuum after the various treatments (oxygen and hydrogen).Injection of reaction liquid Ar purge after the reaction cell, immersed in an oil bath 303 K, started the reaction. Addition reaction in the 5 by bubbling hydrogen in cc/min, stirred by using magnetic Stadler. Also reaction solution substrate octane 1 mM, solvent methanol biphenyls would be 5 ml the analysis standard substances used after stirring for ten minutes at magnetic Stadler 0.65 mM. take in reaction to 1 h, 2 h, 4 h after removing the catalyst in a syringe filter autoinjector for sample tubes into, analyzed the ingredients. And using a GC analysis of the reaction mixture shown to 2.5.3.

ผลลัพธ์ (อังกฤษ) 2:

I using a transparent Pyrex reaction cell in the catalytic reaction. The ribbon 5 cm that was heat-treated at each temperature was HF treatment, it was washed with distilled water, transferred to the reaction cell, after being sufficiently dried in a vacuum, was carried out various processes (oxygen-hydrogen treatment).
After the Ar purge of the reaction cell, the reaction solution was poured, and the reaction was initiated by immersing in an oil bath at 303 K. In addition during the reaction was bubbled hydrogen at 5 cc / min, and the mixture was stirred using a magnetic stirrer. The reaction solution was used after stirring for 10 minutes at a substrate octene 1 mM of methanol 5 ml of the solvent, the magnetic stirrer biphenyl 0.65 mM as a standard analysis. 1 h, 2 h, 4 were removed h after the reaction solution by syringe and transferred to a sample tube for autoinjector and the catalyst was removed with a syringe filter and analyzed for ingredients.
And in the analysis of the reaction solution was used GC shown in 2.5.3.

ผลลัพธ์ (อังกฤษ) 3:

Using transparent as a catalyst in the reaction cell Pyrex. After heat treatment at different temperatures HF ribbon 5 cm, washing with distilled water, the reaction cell after vacuum drying, (oxygen and hydrogen process). After Ar purging of cells injected into the reaction, the reaction liquid and reaction oil soaked in the beginning of K bus 303. Note that in the reaction with hydrogen to 5 cc / min, stirring and bubbling with magnetic stirrer. The reaction solution, mM substrate 1 octeneWith 5 ml of methanol solvent, 0.65 mM biphenyl and analysis of standard substance for 10 minutes in a magnetic stirrer stir after use. 1H, 2h, 4h after the reaction liquid syringe, syringe filter to sample auto injector tube for removing catalyst were analyzed. At the reaction solution and analysis using GC shown in 2.5.3. At